Synthesis of symmetrical and unsymmetrical bis(pyrrolo[2,3-d]pyrimidinyl)methanes

Sharma Meenakshi; Bhuyan Pulak J.

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Synthesis of symmetrical and unsymmetrical bis(pyrrolo[2,3-d]pyrimidinyl)methanes

机译：对称和不对称双（吡咯并[2,3-d]嘧啶基）甲烷的合成

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Some novel symmetrical bis(pyrrolo[2,3-d]pyrimidinyl)methanes were synthesized via diheteroarylation of sp(3) CH bond of acetophenones with molecular iodine and DMSO. Further, an efficient reaction protocol was developed with which both symmetrical and some novel unsymmetrical bis(pyrrolo[2,3-d] pyrimidinyl)methanes were synthesized. For this purpose, we have exploited the highly reactive and good leaving nature of 1,3-dimethylbarbituric acid.

机译：通过将苯乙酮的sp（3）CH键与分子碘和DMSO进行二杂芳基化反应，合成了一些新颖的对称双（吡咯并[2,3-d]嘧啶基）甲烷。此外，开发了一种有效的反应方案，通过该方案可以合成对称和一些新的不对称双（吡咯并[2,3-d]嘧啶基）甲烷。为此，我们利用了1,3-二甲基巴比妥酸的高反应性和良好的离去性质。

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《RSC Advances》 |2014年第105期|共8页
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Sharma Meenakshi; Bhuyan Pulak J.;
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1. Synthesis of symmetrical and unsymmetrical bis(pyrrolo[2,3-d]pyrimidinyl)methanes [J] . Sharma Meenakshi, Bhuyan Pulak J. RSC Advances . 2014,第105期

机译：对称和不对称双（吡咯并[2,3-d]嘧啶基）甲烷的合成
2. A fast and highly efficient protocol for synthesis of pyrrolo[2,3-d] isoxazoles and a new series of novel benzyl bis-pyrrolo[2,3-d]isoxazoles using task-specific ionic liquids as catalyst and green solvent [J] . Rajanarendar E., Raju S., Siva Rami Reddy A., Chemical and Pharmaceutical Bulletin . 2010,第6期

机译：使用任务专用离子液体作为催化剂和绿色溶剂合成吡咯并[2,3-d]异恶唑和一系列新的新型苄基双吡咯并[2,3-d]异恶唑的快速高效方案
3. A Fast and Highly Efficient Protocol for Synthesis of Pyrrolo[2,3-d]isoxazoles and a New Series of Novel Benzyl Bis-pyrrolo[2,3-d]isoxazoles Using Task-Specific Ionic Liquids as Catalyst and Green Solvent [J] . Chemical and Pharmaceutical Bulletin . 2010,第6期

机译：使用任务专用离子液体作为催化剂和绿色溶剂合成吡咯并[2,3-d]异恶唑和一系列新型苄基双吡咯并[2,3-d]异恶唑的快速高效方案
4. SYNTHESIS OF OCTAHYDRO-PYRROLO3,4-b-PIPIREDIN-2-ONES, OCTAHYDRO-PYRROLO3,4-bAZEPIN-2-ONES AND REACTIONS WITH THEM(Abstracts) [C] . Valery S Kochubey, Oleg M Shamaev, Oleg G Rodin European Symposium on Organic Chemistry . 2007

机译：八氢盐 - 吡咯的合成3,4-B - 哌啶-2-吡咯3,4-B偶氮二蛋白-2-β-2 - 与它们（摘要）
5. Synthesis of substituted pyrrolo[2,3-d]pyrimidines as microtubule-binding agents and HSP90 inhibitors [D] . Lin, Lu 2013

机译：取代吡咯并[2,3-d]嘧啶类化合物作为微管结合剂和HSP90抑制剂的合成
6. Symmetrically and Unsymmetrically Bridged Methylenebis(allopurinols): Synthesis of Dimeric Potential Anti-Gout Drugs [O] . Helmut Rosemeyer, Martina Anders, Frank Seela 2007

机译：对称和不对称桥联的亚甲基双（aluropurinols）：二聚体潜在的抗痛风药的合成。
7. Preparation, characterization, and catalytic application of metallic nanocrystalline MgAl2O4 in the synthesis of 3-hydroxy-3-indolyl-indolin-2-ones, symmetrical and unsymmetrical 3,3′-bis(indolyl)indolin-2-ones, and 3,3′-bis(indolyl)methanes [O] . Nikoofar Kobra, Haghighi Maryam, Khademi Zahra 2016

机译：金属纳米晶体MgAl2O4的制备，表征和催化应用，用于合成3-羟基-3-吲哚基-吲哚-2-酮，对称和不对称的3,3'-双（吲哚基）吲哚-2-酮和3， 3'-双（吲哚基）甲烷

Synthesis of symmetrical and unsymmetrical bis(pyrrolo[2,3-d]pyrimidinyl)methanes

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