Pd/mannose promoted tandem cross coupling-nitro reduction: expedient synthesis of aminobiphenyls and aminostilbenes

Rohilla Sandeep; Pant Pradeep; Jain Nidhi

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Pd/mannose promoted tandem cross coupling-nitro reduction: expedient synthesis of aminobiphenyls and aminostilbenes

机译：钯/甘露糖促进串联交叉偶联-硝基还原：氨基联苯和氨基苯乙烯的简便合成

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The dual role of D-mannose as a ligand for Pd catalyzed cross-coupling, and as a hydrogen source for nitro reduction is demonstrated in a modular cross coupling-nitro reduction sequence. The synthetic utility and generality of this green protocol has been illustrated by the synthesis of 20 aminobiphenyl and 10 aminostilbene derivatives in high yields through a one-pot Suzuki coupling-nitro reduction and a Heck coupling-nitro reduction, respectively, starting from halonitroarenes as substrates.

机译：D-甘露糖作为钯催化的交叉偶联的配体，以及作为硝基还原的氢源的双重作用已在模块化交叉偶联-硝基还原序列中得到证实。该绿色方案的合成用途和普遍性已通过以卤代硝基芳烃为底物，分别通过一锅Suzuki偶联-硝基还原和Heck偶联-硝基还原以高收率合成20个氨基联苯和10个氨基二苯乙烯衍生物得到了说明。。

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《RSC Advances》 |2015年第40期|共7页
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Rohilla Sandeep; Pant Pradeep; Jain Nidhi;
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1. Pd/mannose promoted tandem cross coupling-nitro reduction: expedient synthesis of aminobiphenyls and aminostilbenes [J] . Rohilla Sandeep, Pant Pradeep, Jain Nidhi RSC Advances . 2015,第40期

机译：钯/甘露糖促进串联交叉偶联-硝基还原：氨基联苯和氨基苯乙烯的简便合成
2. Expedient one-pot synthesis of indolo[3,2-c]isoquinolines via a base-promoted N-alkylation/tandem cyclization [J] . Nguyen Huy H., Fettinger James C., Haddadin Makhluf J., Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2015,第40期

机译：通过碱促进的N-烷基化/串联环化方便地一锅合成吲哚[3,2-c]异喹啉
3. An imidazolium-based organopalladium-functionalized organic-inorganic hybrid silica promotes one-pot tandem Suzuki cross coupling-reduction of haloacetophenones and arylboronic acids [J] . Zhang Dacheng, Cheng Tanyu, Liu Guohua Applied Catalysis, B. Environmental: An International Journal Devoted to Catalytic Science and Its Applications . 2015,第Null期

机译：咪唑基有机钯官能化的有机-无机杂化二氧化硅可促进一锅串联Suzuki交叉偶联还原卤代苯乙酮和芳基硼酸
4. A study of planar jet flow control and perforated fairings for the reduction of the flow-induced noise of tandem rods in a cross-flow [C] . Kun Zhao, Patrick N. Okolo, John Kennedy, AIAA/CEAS aeroacoustics conference . 2016

机译：平面射流控制和带孔整流罩的研究，用于减少横流中的串联杆的流动引起的噪声
5. Macrocyclization through ene-yne cross-coupling/alkyne reduction tandem reaction and its application in natural product synthesis. [D] . Li, Wei. 2015

机译：通过烯-炔交叉偶联/炔烃还原串联反应进行大环化及其在天然产物合成中的应用。
6. Expedient one-pot synthesis of indolo32-cisoquinolines via a base-promoted N–alkylation/tandem cyclization [O] . Huy H. Nguyen, James C. Fettinger, Makhluf J. Haddadin, -1

机译：通过碱促进的N-烷基化/串联环化方便地一锅合成吲哚32-c异喹啉
7. Expedient one-pot synthesis of indolo3,2-cisoquinolines via a base-promoted N-alkylation/tandem cyclization [O] . Huy H. Nguyen, James C. Fettinger, Makhluf J. Haddadin, 2015

机译：通过碱基促进的N-烷基化/串联环化的Indolo 3,2-C异喹啉的有利1罐合成

Pd/mannose promoted tandem cross coupling-nitro reduction: expedient synthesis of aminobiphenyls and aminostilbenes

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