Regiospecific cyclization of 4-alkoxyvinyl trifluoro[chloro]methyl ketones with 6-trifluoro[chloro]methyl-2-hydrazine pyrimidines. A convenient method to obtain trifluoro[chloro]methylated 2-(5-hydroxy-5-trifluoro[chlorolmethyl-4,5-dihydro-1H-pyrazol

Zanatta N.; Flores DC.; Madruga CC.; Faoro D.; Flores AFC.; Bonacorso HG. Martins MAP.

首页> 外文期刊>Synthesis: International Journal of Methods in Synthetic Organic Chemistry >Regiospecific cyclization of 4-alkoxyvinyl trifluoro[chloro]methyl ketones with 6-trifluoro[chloro]methyl-2-hydrazine pyrimidines. A convenient method to obtain trifluoro[chloro]methylated 2-(5-hydroxy-5-trifluoro[chlorolmethyl-4,5-dihydro-1H-pyrazol

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Regiospecific cyclization of 4-alkoxyvinyl trifluoro[chloro]methyl ketones with 6-trifluoro[chloro]methyl-2-hydrazine pyrimidines. A convenient method to obtain trifluoro[chloro]methylated 2-(5-hydroxy-5-trifluoro[chlorolmethyl-4,5-dihydro-1H-pyrazol

机译：4-烷氧基乙烯基三氟[氯]甲基酮与6-三氟[氯]甲基-2-肼嘧啶的区域特异性环化。一种获得三氟[氯]甲基化的2-（5-羟基-5-三氟[氯甲基--4,5-二氢-1H-吡唑]的简便方法

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The regiospecific synthesis of a novel series of 4-trifluoro[chloro]-2-(5-hydroxy-5-trifluoro[chloro]methyl-4,5-dihydro-1H- pyrazol-1-yl]-pyrimidines from the reactions of 4-alkoxy-1,1,1-trifluoro[chloro]-alk-3-en-2-ones with 6-trifluoro[chloro]methy]-2-hydrazine pyrimidines is presented. [References: 45]

机译：新型的4-三氟[氯] -2-（5-羟基-5-三氟[氯]甲基-4,5-二氢-1H-吡唑-1-基]-嘧啶的区域特异性合成提出了带有6-三氟[氯]甲基] -2-肼嘧啶的4-烷氧基-1,1,1-三氟[氯]-烷-3-烯-2-酮[参考文献：45]

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来源
《Synthesis: International Journal of Methods in Synthetic Organic Chemistry》 |2003年第6期|共5页
作者
Zanatta N.; Flores DC.; Madruga CC.; Faoro D.; Flores AFC.; Bonacorso HG. Martins MAP.;
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正文语种 eng
中图分类有机化学;
关键词
Pyrazolylpyrimidines; Pyrazoles; Pyrimidines; Halogenated heterocycles; Haloacetylated enol ethers; Alkoxyvinyl trihalomethyl ketones; One-pot synthesis; Trifluoromethyl ketones; Derivatives; Reagents; Systems; Agents;

机译：吡唑基嘧啶;吡唑;嘧啶;卤代杂环;卤代乙酰化的烯醇醚;烷氧基乙烯基三卤代甲基酮;一锅合成;三氟甲基酮;衍生物;试剂;体系;试剂;

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1. Regiospecific cyclization of 4-alkoxyvinyl trifluoro[chloro]methyl ketones with 6-trifluoro[chloro]methyl-2-hydrazine pyrimidines. A convenient method to obtain trifluoro[chloro]methylated 2-(5-hydroxy-5-trifluoro[chlorolmethyl-4,5-dihydro-1H-pyrazol [J] . Zanatta N., Flores DC., Madruga CC., Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2003,第6期

机译：4-烷氧基乙烯基三氟[氯]甲基酮与6-三氟[氯]甲基-2-肼嘧啶的区域特异性环化。一种获得三氟[氯]甲基化的2-（5-羟基-5-三氟[氯甲基--4,5-二氢-1H-吡唑]的简便方法
2. 2-{1-[2-((2-Ammonioethyl){2-[1-(5-chloro-2-hydroxyphenyl)ethylideneamino]ethyl}amino)ethyliminio]ethyl}-4-chlorophenolate trifluoroacetate [J] . Ali H.M., Lee S.M., Lo K.M., Acta Crystallographica Section E: Crystallographic Communications . 2009,第2期

机译：2- {1- [2-（（2-氨基碘乙基）} {2- [1-（5-氯-2-羟基苯基）亚乙基氨基]乙基}氨基}乙基亚氨基乙基} -4-氯酚盐三氟乙酸盐
3. 1-Methyl-3-trifluoromethyl-5-[(3-chlorophenyl)sulfanyl]-1H-pyrazole-4-carbaldehyde O-(4-chlorobenzoyl)oxime [J] . Dai H., Luo K.-P., Shi L., Acta Crystallographica Section E: Crystallographic Communications . 2011,第12期

机译：1-甲基-3-三氟甲基-5-[（3-氯苯基）硫烷基] -1H-吡唑-4-甲醛O-（4-氯苯甲酰基）肟
4. 5-(3-Chlorophenylsulfanyl)-1-methyl-3-trifluoromethyl-1H-pyrazole-4-carbaldehyde O-(2-chloro-13-thiazol-5-yl)methyloxime [O] . Hong Dai, Shuang Li, Kun-Peng Luo, 2012

机译：5-（3-氯苯甲酰基硫烷基）-1-甲基-3-三氟甲基-1H-吡唑-4-甲醛O-（（2-氯-13-噻唑-5-基）甲基肟
5. 2-{1-[2-((2-Ammonioethyl){2-[1-(5-chloro-2-hydroxyphenyl)ethylideneamino]ethyl}amino)ethyliminio]ethyl}-4-chlorophenolate trifluoroacetate [O] . Lee, See Mun, Ali, Hapipah Mohd., Lo, Kong Mun, 2009

机译：2- {1- [2-（（2-氨基碘乙基）} {2- [1-（5-氯-2-羟基苯甲基）乙基亚乙基氨基]乙]基}氨基）乙基亚氨基基} -4-氯酚盐三氟ate乙酸盐
6. Initial Submission: Teratology Study of 3-Chloro-N-(5-Chloro- 2,6-dinitro-4-Trifluoro- Methyl-Phenyl) 5-Trifluoro-Methyl-Pyridinamine in Rats with Cover Letter dated 08/19/1992 [R] . 1992

机译：初步提交：大鼠的3-氯-N-（5-氯-2,6-二硝基-4-三氟 - 甲基 - 苯基）-5-三氟甲基 - 吡啶胺的畸形学研究，日期为1990年8月19日

Regiospecific cyclization of 4-alkoxyvinyl trifluoro[chloro]methyl ketones with 6-trifluoro[chloro]methyl-2-hydrazine pyrimidines. A convenient method to obtain trifluoro[chloro]methylated 2-(5-hydroxy-5-trifluoro[chlorolmethyl-4,5-dihydro-1H-pyrazol

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