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Evaluation of freezing pre-treatments for the lyophilisation of apple

机译:苹果冷冻干燥的冷冻预处理评估

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The effect of freezing rate on the quality of dried Jonagold and Idared (Malus domestica Borkh.) was studied. Apple slices underwent various pre-treatments, i.e. freezing in household freezer (freezing speed/rate: 0,5?C/min), contact plate freezing (2?C/min) and vacuumfreezing (3?C/min). The quality of the freeze-dried product was then evaluated in terms of water activity (aw), hardness, color and rehydration. The texture and color experiments were carried out with texture analyser and colorimeter. The aw of apple slices was measured by aw apparatus. It was found that drying time was influenced by freezing rate. The freezing in household freezer (slow freezing rate) significantly reduces the duration of the freeze-drying process and consequently the process costs. The slow freezing rate allows the growth of large ice crystals at the beginning of the freeze-drying process; this fact should consequently lead to larger pores and injured cell walls and thus to shorter freeze-drying time. Quality of the freezing in household freezer product was assessed as higher than the quality of the other freezing pre-treated material. Slow freezing rate resulted softer texture and higher rehydration capacity than that of other pre-treated samples. In all cases, slow freezing speed lead to lower final moisture content, total color difference and water activity. Freeze-dried samples prepared with higher freezing rates (3?C/min) were the most white in color because small pores, originated by sublimation of small ice crystals formed by fast freezing.
机译:研究了冷冻速度对干燥的乔纳金和伊达雷德(Malus domestica Borkh。)品质的影响。苹果片经过了各种预处理,即在家用冰箱中冷冻(冷冻速度/速率:0.5?C / min),接触板冷冻(2?C / min)和真空冷冻(3?C / min)。然后根据水活度(aw),硬度,颜色和补水来评估冷冻干燥产品的质量。用纹理分析仪和色度计进行纹理和颜色实验。苹果片的aw用aw装置测量。发现干燥时间受冷冻速度的影响。家用冷冻机中的冷冻(缓慢的冷冻速度)显着减少了冷冻干燥过程的持续时间,并因此降低了过程成本。缓慢的冷冻速度使大的冰晶在冷冻干燥过程开始时就可以生长。因此,该事实应导致更大的孔和受损的细胞壁,从而缩短冷冻干燥时间。家用冷冻柜产品的冷冻质量被评估为高于其他冷冻预处理材料的质量。与其他预处理样品相比,缓慢的冷冻速度导致质地更柔软,并具有更高的补液能力。在所有情况下,缓慢的冷冻速度都会导致最终水分含量,总色差和水分活度降低。以较高的冷冻速度(3?C / min)制备的冷冻干燥样品颜色最白,因为小孔是由快速冷冻形成的小冰晶升华而产生的。

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