Synthesis of homophthalates by [3+3] cyclocondensation reactions of 1,3-bis(silyloxy)-1,3-butadienes with silylated methyl 3,5-dioxohexanoate

Hefner J.; Villinger A.; Langer P.

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Synthesis of homophthalates by [3+3] cyclocondensation reactions of 1,3-bis(silyloxy)-1,3-butadienes with silylated methyl 3,5-dioxohexanoate

机译：1,3-双（甲硅烷氧基）-1,3-丁二烯与甲硅烷基化的3,5-二氧己酸甲酯的[3 + 3]环缩合反应合成高邻苯二甲酸酯

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摘要

Homophthalates were prepared by formal [3+3] cyclocondensation of 1,3-bis(silyl enol ethers) with silylated methyl 3,5-dioxohexanoate.

机译：通过将1,3-双（甲硅烷基烯醇醚）与甲硅烷基化的3,5-二氧己酸甲酯进行正式的[3 + 3]环缩合反应，可以制备高邻苯二甲酸酯。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2013年第7期|共5页
作者
Hefner J.; Villinger A.; Langer P.;
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正文语种 eng
中图分类 54;
关键词
Cyclizations; Homophthalates; Regioselectivity; Silyl enol ethers;

机译：环化;高邻苯二甲酸酯;区域选择性;甲硅烷基烯醇醚;

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1. Synthesis of homophthalates by [3+3] cyclocondensation reactions of 1,3-bis(silyloxy)-1,3-butadienes with silylated methyl 3,5-dioxohexanoate [J] . Hefner J., Villinger A., Langer P. Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2013,第7期

机译：1,3-双（甲硅烷氧基）-1,3-丁二烯与甲硅烷基化的3,5-二氧己酸甲酯的[3 + 3]环缩合反应合成高邻苯二甲酸酯
2. Synthesis of functionalized acetophenones by formal [3+3] cyclocondensations of 1,3-bis(silyloxy)-1,3-butadienes with 3-alkoxyand 3-silyloxy-2-acetyl-2-en-1-ones [J] . Dede R., Riahi A., Shkoor M., Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2013,第9期

机译：1,3-双（甲硅烷氧基）-1,3-丁二烯与3-烷氧基和3-甲硅烷氧基-2-乙酰基-2-烯-1-酮的正式[3 + 3]环缩合反应合成官能化的苯乙酮
3. Synthesis of 2-Hydroxy-5-Arylselanyl-Benzoates by [3+3] Cyclocondensation of 1,3-Bis(Silyloxy)-1,3-Butadienes with 2-Arylseleno-3-Silyloxy-Alk-2-en-1-Ones [J] . Mohanad Shkoora Olumide Fatunsina Abdolmajid Riahiab amp, Peter Langerab Phosphorus, Sulfur, and Silicon and the Related Elements . 2011,第9期

机译：1,3-双（甲硅烷基）-1,3-丁二烯与2-芳基硒-3-甲硅烷氧基-烷基-2-en-1-的[3 + 3]环缩合反应合成2-羟基-5-芳基硒烷基-苯甲酸酯那些
4. SIMULTANEOUS CONTROL OF MOLECULAR WEIGHT AND 1,4-C/S-SELECTIVITY IN THE POLYMERIZATION OF 1,3-BUTADIENE WITH N,N'-BIS(3,5-DI-TERT-BUTYL SALICYLIDENE)-1,2-DIPHENYLETHYLENE DIAMINATO COBALT IN COMBINATION WITH DIETHYLALUNINUM CHLORIDE [C] . Kiyoshi Endo, Kenji Nakatani Technical Meeting of the rubber division,American Chemical Society . 2009

机译：用N，N'-BIS（3,5-二叔丁基水杨烯）-1,2-二苯基乙烯二氨基氨基聚合，同时对分子量和1,4-C / S选择性的控制在1,3-丁二烯中的聚合中钴与二乙基氯化物组合
5. Products and mechanisms of the reactions of chlorine atoms with 1,3-butadiene and 2-methyl-1,3-butadiene (Isoprene) in air at room temperature. [D] . Wang, Wezhong. 2000

机译：室温下空气中氯原子与1,3-丁二烯和2-甲基-1,3-丁二烯（异戊二烯）反应的产物和机理。
6. First synthesis of 4-(arylsulfonyl)phenols by regioselective 3+3 cyclocondensations of 13-bis(silyloxy)-13-butadienes with 2-arylsulfonyl-3-ethoxy-2-en-1-ones [O] . Abdolmajid Riahi, Mohanad Shkoor, Olumide Fatunsin, -1

机译：13-双（甲硅烷氧基）-13-丁二烯与2-芳基磺酰基-3-乙氧基-2-烯-1-酮的区域选择性3 + 3环缩合反应首次合成4-（芳基磺酰基）苯酚
7. First synthesis of 4-(arylsulfonyl)phenols by regioselective 3+3 cyclocondensations of 1,3-bis(silyloxy)-1,3-butadienes with 2-arylsulfonyl-3-ethoxy-2-en-1-ones [O] . Abdolmajid Riahi, Mohanad Shkoor, Olumide Fatunsin, 2009

机译：首先合成4-（芳基磺酰基）酚，通过区域选择性3 + 3环形致残的1,3-双（甲硅烷基氧基）-1,3-丁二烯，具有2-芳基磺酰基-3-乙氧基-2-烯-1-烯-1-烯
8. Epoxidation of E-1,4-poly(2-triethylsilyl-1,3-butadiene) and E-1,4-poly-(2,3-bis(trimethylsilyl)-1,3-butadiene). Stereochemical analysis of E-1,4-poly(2,3-epoxy-2-triethylsilyl-1,3-butadiene) and E-1,4-poly-(2,3-bis(trimethylsilyl [R] . Jiang, W., Weber, W. P. 1988

机译：E-1,4-聚（2-三乙基甲硅烷基-1,3-丁二烯）和E-1,4-聚 - （2,3-双（三甲基甲硅烷基）-1,3-丁二烯）的环氧化。 E-1,4-聚（2,3-环氧-2-甲基甲硅烷基-1,3-丁二烯）和E-1,4-聚 - （2,3-双（三甲基甲硅烷基）的立体化学分析

Synthesis of homophthalates by [3+3] cyclocondensation reactions of 1,3-bis(silyloxy)-1,3-butadienes with silylated methyl 3,5-dioxohexanoate

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