Crystal structure of 1, 3-di-2-[(4-methoxyphenyl)-1-diazenyl]imidazolidine

Kumar Biradha; Hilary Jenkins; M. Brad Peori; Keith Vaughan; Michael J. Zaworotko

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Crystal structure of 1, 3-di-2-[(4-methoxyphenyl)-1-diazenyl]imidazolidine

机译：1，3-二-2-[[（4-甲氧基苯基）-1-二氮烯基]咪唑烷的晶体结构

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The crystal and molecular structure of 1, 3-di-2-[(4-methoxyphenyl)-1-diazenyl]imidazolidine (1) has been determined by single crystal X-ray diffraction analysis. This novel bis-triazene assumes a close-to planar structure with the aryltriazene moieties aligned in diametrically opposed directions, unlike many other previously reported bis-triazenes, which assume a folded structure. The structure of 1 is compared with the closely related, non-cyclic bis-triazene analogue (2), and also compared with the structure of the simple mono-triazene (3). Crystal data: 1 C_(17)H_(20)N_6O_2, monoclinic, space group C2/c, a = 34.948(3), b = 5. 925(5), c = 8.1225(6) A, #beta# = 100.8420(10) deg, and V = 1652.0(2) A~3, for Z = 4.

机译：1，3-二-2-[（4-甲氧基苯基）-1-二氮烯基]咪唑烷（1）的晶体和分子结构已经通过单晶X射线衍射分析确定。与许多先前报道的双三叠氮烯呈折叠结构不同，该新颖的双三叠氮烯具有接近于平面的结构，其中芳基三叠氮烯部分沿沿直径相反的方向排列。将1的结构与紧密相关的非环状双三氮烯类似物（2）进行比较，还将其与简单的单三氮烯（3）的结构进行比较。晶体数据：1 C_（17）H_（20）N_6O_2，单斜晶，C2 / c空间群，a = 34.948（3），b = 5. 925（5），c = 8.1225（6）A，＃beta＃= 100.8420（10）度，V = 1652.0（2）A〜3，Z = 4。

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《Journal of chemical crystallography》 |1999年第9期|共5页
作者
Kumar Biradha; Hilary Jenkins; M. Brad Peori; Keith Vaughan; Michael J. Zaworotko;
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正文语种 eng
中图分类晶体学;
关键词
crystal structure; imidazolidine; triazene; bis-triazene; methoxy substituent; pi; -; pi; stacking;

机译：晶体结构;咪唑烷;三氮烯;双三氮烯;甲氧基取代基;pi;-;pi;堆积;

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1. Crystal structure of 1, 3-di-2-[(4-methoxyphenyl)-1-diazenyl]imidazolidine [J] . Kumar Biradha, Hilary Jenkins, M. Brad Peori, Journal of chemical crystallography . 1999,第9期

机译：1，3-二-2-[[（4-甲氧基苯基）-1-二氮烯基]咪唑烷的晶体结构
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Crystal structure of 1, 3-di-2-[(4-methoxyphenyl)-1-diazenyl]imidazolidine

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