A facile, one-pot procedure for the conversion of aromatic aldehydes to esters, as well as thioesters and amides, via acyl hydrazide intermediates

Maruani Antoine; Lee Maximillian T. W.; Watkins George; Akhbar Ahmed R.; Baggs Henry; Shamsabadi Andre; Richards Daniel A.; Chudasama Vijay

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A facile, one-pot procedure for the conversion of aromatic aldehydes to esters, as well as thioesters and amides, via acyl hydrazide intermediates

机译：通过酰基酰肼中间体将芳香醛转化为酯，以及硫代酰酯和酰胺的容易的单罐方法

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摘要

Herein we present an efficient method for the synthesis of esters from aromatic aldehydes via readily accessible acyl hydrazides. The developed reaction protocol is shown to be tolerant of a range of aromatic aldehydes, bearing various functionalities, as well as being amenable to the synthesis of thioesters and amides.

机译：在此，我们通过易于可偏转的酰基酰肼来提出一种优化的方法，用于通过易于可偏转的酰基酰肼来合成来自芳族醛的酯。显示出开发的反应方案被证明是耐受一系列芳香族醛，携带各种函数的耐受性，以及含有硫酯和酰胺的合成。

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《RSC Advances》 |2016年第4期|共5页
作者
Maruani Antoine; Lee Maximillian T. W.; Watkins George; Akhbar Ahmed R.; Baggs Henry; Shamsabadi Andre; Richards Daniel A.; Chudasama Vijay;
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UCL Dept Chem London WC1H 0AJ England;

UCL Dept Chem London WC1H 0AJ England;

UCL Dept Chem London WC1H 0AJ England;

UCL Dept Chem London WC1H 0AJ England;

UCL Dept Chem London WC1H 0AJ England;

UCL Dept Chem London WC1H 0AJ England;

UCL Dept Chem London WC1H 0AJ England;

UCL Dept Chem London WC1H 0AJ England;

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正文语种 eng
中图分类化学;
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1. A facile, one-pot procedure for the conversion of aromatic aldehydes to esters, as well as thioesters and amides, via acyl hydrazide intermediates [J] . Maruani Antoine, Lee Maximillian T. W., Watkins George, RSC Advances . 2016,第4期

机译：通过酰基酰肼中间体将芳香醛转化为酯，以及硫代酰酯和酰胺的容易的单罐方法
2. Conversions of Coumarins Accompanied by Intermediate Opening and Recyclization of the Lactone Ring. 2. Study of the Interaction of Malonic Acid Hydrazide and Amide Derivatives with 3-Acyl(3-cyano, 3-ethoxycarbonyl)Coumarins [J] . M. P. Nemeryuk, V. D. Dimitrova, O. S. Anisimova, Chemistry of heterocyclic compounds . 2005,第10期

机译：内酯环的中间打开和再循环伴随香豆素的转化。 2.丙二酸酰肼和酰胺衍生物与3-酰基（3-氰基，3-乙氧基羰基）香豆素相互作用的研究
3. One-pot two-step conversion of aromatic carboxylic acids and esters to aromatic aldehydes via indium-catalyzed reductive thioacetalization and desulfurization [J] . Sakai Norio, Minato Kohei, Ogiwara Yohei Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2017,第48期

机译：通过催化催化的还原硫代缩醛化和脱硫芳族羧酸和酯对芳香族醛的一锅两步转化
4. Backbone amide linker (BAL)/fmoc synthesis of peptide thioester intermediates required for native chemical ligation [C] . Dominique Lelievre, George Barany the International Peptide Symposium . 2001

机译：骨干酰胺链接剂（BAL）/ FMOC本土化学连接所需的肽硫酯中间体
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. Rhodium‐Catalyzed Decarbonylative Borylation of Aromatic Thioesters for Facile Diversification of Aromatic Carboxylic Acids [O] . Dr. Hidenori Ochiai, Dr. Yuta Uetake, Dr. Takashi Niwa, -1

机译：铑催化的芳族硫代酸酯的脱羰基硼化反应可轻松实现芳族羧酸的多样化
7. A facile, one-pot procedure for the conversion of aromatic aldehydes to esters, as well as thioesters and amides, via acyl hydrazide intermediates [O] . Antoine Maruani, Maximillian T. W. Lee, George Watkins, 2016

机译：通过酰基酰肼中间体将芳香醛转化为酯，以及硫代酰酯和酰胺的容易的单罐方法

A facile, one-pot procedure for the conversion of aromatic aldehydes to esters, as well as thioesters and amides, via acyl hydrazide intermediates

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