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Identification of the Intermetallic Compound Layer Formed at the Interface of Roll-Bonded Aluminum-Clad Steel by Thermal Annealing

机译:热退火对轧制结合铝包钢界面形成的金属间化合物层的识别

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摘要

Aluminum clad steel (ACS) is an excellent layered composite material. An intensive investigation into roll-bonded ACS was carried out to identify the intermetallic compound (IMC) formed at the interface between the aluminum (Al) and the steel. A series of analyzing methods was applied to the IMC layer formed at the interface during annealing at 540 °C for 16 h. An electron probe micro-analyzer (EPMA) measured a value of 28.5 atomic percent for the Fe in the IMC layer, which coincided with the Fe_2Al_5 phase. An analysis of the X-ray diffraction pattern for the IMC layer in the ACS materials showed a very strong peak for the (002) plane of Fe_2Al_5. Vickers microhardness testing of the IMC layer revealed a very high value (1,110 Hv). The results of EPMA, XRD and microhardness values verified that the IMC layer in the sample that had been annealed at 540 °C for 16 h was the Fe_2Al_5 phase.
机译:铝包钢(ACS)是一种出色的层状复合材料。对轧制ACS进行了深入研究,以确定在铝(Al)和钢之间的界面处形成的金属间化合物(IMC)。在540°C退火16 h期间,对界面处形成的IMC层采用了一系列分析方法。电子探针微分析仪(EPMA)在IMC层中测得的Fe值为28.5原子百分比,与Fe_2Al_5相一致。 ACS材料中IMC层的X射线衍射图分析表明,Fe_2Al_5的(002)平面有很强的峰。 IMC层的维氏显微硬度测试显示出非常高的值(1,110 Hv)。 EPMA,XRD和显微硬度值的结果证明,在540°C退火16 h的样品中的IMC层为Fe_2Al_5相。

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