Synthesis of beta-ketoesters from renewable resources and Meldrum's acid

Brinkerhoff Rafael C.; Tarazona Hernan F.; de Oliveira Patrick M.; Flores Darlene C.; Montes DOca Caroline Da R.; Russowsky Dennis; Montes DOca Marcelo G.

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Synthesis of beta-ketoesters from renewable resources and Meldrum's acid

机译：由可再生资源和梅德鲁姆酸合成β-酮酸酯

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beta-Ketoesters are valuable building blocks for the synthesis of compounds with different biological activities. In this study, a series of fatty beta-ketoesters were obtained from fatty acids and Meldrum's acid using N,N-dicyclohexylcarbodiimide and dimethylaminopyridine. In addition, we demonstrate for the first time the synthesis of new fatty beta-ketoesters from oleic (cis-C18:1), elaidic (trans-C18:1), ricinoleic (cis-C18:1, 12-OH), linoleic (cis, cis-C18:2), and linolenic (cis, cis, cis-C18:3) acids in good yields.

机译：β-酮酸酯是合成具有不同生物活性的化合物的重要基础。在这项研究中，使用N，N-二环己基碳二亚胺和二甲基氨基吡啶，从脂肪酸和Meldrum酸中获得了一系列脂肪β-酮酸酯。此外，我们首次证明了从油酸（顺式-C18：1），亚麻酸（反式-C18：1），蓖麻油酸（顺式-C18：1，12-OH），亚油酸合成新的脂肪β-酮酸酯（顺式，顺式-C18：2）和亚麻酸（顺式，顺式，顺式-C18：3）酸，收率高。

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《RSC Advances》 |2014年第91期|共4页
作者
Brinkerhoff Rafael C.; Tarazona Hernan F.; de Oliveira Patrick M.; Flores Darlene C.; Montes DOca Caroline Da R.; Russowsky Dennis; Montes DOca Marcelo G.;
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1. Synthesis of beta-ketoesters from renewable resources and Meldrum's acid [J] . Brinkerhoff Rafael C., Tarazona Hernan F., de Oliveira Patrick M., RSC Advances . 2014,第91期

机译：由可再生资源和梅德鲁姆酸合成β-酮酸酯
2. Synthesis of Biobased Polyurethane from Oleic and Ricinoleic Acids as the Renewable Resources via the AB-Type Self-Condensation Approach [J] . Dnyaneshwar V. Palaskar, Aurelie Boyer, Eric Cloutet Biomacromolecules . 2010,第5期

机译：通过AB型自缩合方法，以油酸和蓖麻油酸为可再生资源合成生物基聚氨酯
3. Biodegradable Polymers Based on Renewable Resources.V.Synthesis and Biodegradation Behavior of Poly(ester amide)s Composed of 1,4:3,6-Dianhydro-D-glucitol,#alpha#-Amino Acid,and Aliphatic Dicarboxylic Acid Units [J] . Masahiko Okada, Masashi Yamada, Makito Yokoe, Journal of Applied Polymer Science . 2001,第11期

机译：五，由1,4：3,6-二氢-D-葡萄糖醇，＃α＃-氨基酸和脂肪族二羧酸单元组成的聚酯（酯酰胺）的合成与生物降解行为
4. THE USE OF POLYESTER POLYOLS BASED ON POLYMERIZED FATTY ACIDS FROM RENEWABLE RESOURCES IN POLYURETHANE AND UV CURABLE APPLICATIONS [C] . William McNamee, Erwin Honcoop Annual international waterborne, high-solids, and powder coatings symposium;International waterborne, high-solids, and powder coatings symposium . 2011

机译：基于可再生资源的聚合脂肪酸的聚酯多元醇在聚氨酯中的应用以及可紫外线固化的应用
5. Synthesis of comb-like copolymers from renewable resources: Itaconic anhydride, stearyl methacrylate and lactic acid. [D] . Shang, Shurui. 2009

机译：由可再生资源合成衣梳状共聚物：衣康酸酐，甲基丙烯酸十八烷基酯和乳酸。
6. Effective Synthesis Route for Linear and Cross-LinkedBiodegradable Polyesters Using Aliphatic Meldrum’s Acid Derivativesas Monomers [O] . Liang-Kai Lin, Jane Wang, Ying-Ling Liu, 2018

机译：线性和交联的有效合成路线使用脂肪族麦德鲁姆酸衍生物的可生物降解聚酯作为单体
7. Synthesis and Characterization of All Renewable Resources Based Branched Polyester: Poly(2,5-furandicarboxylic acid-co-glycerol) [O] . Ananda S. Amarasekara, Ashfaqur Razzaq, Paul Bonham 2013

机译：所有可再生资源的支化聚酯的合成与表征：聚（2,5-呋喃羧酸 - 共甘油）
8. Biosynthesis of long-chain dicarboxylic acid monomers from renewable resources.211 Final technical report [R] . Mobley, D. P. 1999

机译：来自可再生资源的长链二羧酸单体的生物合成.211最终技术报告

Synthesis of beta-ketoesters from renewable resources and Meldrum's acid

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